HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-4-dimethylamino-2-methoxybenzoic acid → HCID 14881853, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-4-dimethylamino-2-methoxybenzoic acid | HCID 11075202 | — |
| Reactant | 4-[3-(4-Chlorophenoxy)propyl]-2-morpholinemethanamine | HCID 14881852 | — |
| Product | HCID 14881853 | HCID 14881853 | — |
Reaction Steps
The hemihydrate of the title compound is prepared in substantially the same manner as in Example 6(1), using 2-aminomethyl-4-[3-(4-chlorophenoxy)propyl]morpholine and 5-chloro-4-dimethylamino-2-methoxybenzoic acid, respectively, in place of 2-aminomethyl-4-(4-cyanobenzyl)morpholine and 4-amino-5-chloro-2-methoxybenzoic acid in Example 6(1), mp 128°-130° C. (recrystallized from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870074 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-6878f2d6e25442dca34028244df17091 |
| Source note | uspto-grants-1989_09 |