反应详情

2-Acetylaminomethyl-4-benzylmorpholine (120 g) is dissolved in a mixture of ethanol (1000 ml) and acetic acid (30 ml) and hydrogenated over 10% palladium on carbon (5 g) at about 60° C. After the calculated amount of the hydrogen is absorbed, the catalyst is filtered off. The filtrate is evaporated under reduced pressure to give the title compound as an oil.

1. customAfter the calculated amount of the hydrogen is absorbed
2. filtrationthe catalyst is filtered off
3. customThe filtrate is evaporated under reduced pressure