HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14882034, compound → HCID 19848620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14882034 | HCID 14882034 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19848620 | HCID 19848620 | 98.8% |
Reaction Steps
A solution of 2-(2-cyanoethyl)-4-benzyloxycarbonylmorpholine (10.7 g) in ethanol (60 ml) is hydrogenated over 5% palladium on carbon (1 g) at 25° C. After the calculated amount of hydrogen is absorbed, the catalyst is filtered off. The filtrate is evaporated under reduced pressure to give the title compound (5.4 g) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870074 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-a1e2b18fd18e45feb9bf85c08b75f2de |
| Source note | uspto-grants-1989_09 |