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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1608224Generated: November 2, 2026

HCID 19848614, compound → HCID 14881837, compound

https://huagongshe.com/reaction/1608224

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19848614HCID 19848614—
CatalystNickelHCID 935—
SolventEthanolHCID 702—
SolventAzane;hydrateHCID 12896473—
ProductHCID 14881837HCID 1488183786%

Reaction Steps

A solution of 2-(2-cyanoethyl)-4-benzylmorpholine (8 g) in a mixture of ethanol (60 ml) and 28% ammonia water (4 ml) is hydrogenated over Raney nickel at 25° C. After the calculated amount of hydrogen is absorbed, the catalyst is filtered off. The filtrate is evaporated under reduced pressure to give the title compound (7 g) as an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04870074
Source datasetuspto-grants-1989_09
ORD IDord-6913707d6d5a4a51b311a2425cfcfefa
Source noteuspto-grants-1989_09