HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19848614, compound → HCID 14881837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19848614 | HCID 19848614 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Azane;hydrate | HCID 12896473 | — |
| Product | HCID 14881837 | HCID 14881837 | 86% |
Reaction Steps
A solution of 2-(2-cyanoethyl)-4-benzylmorpholine (8 g) in a mixture of ethanol (60 ml) and 28% ammonia water (4 ml) is hydrogenated over Raney nickel at 25° C. After the calculated amount of hydrogen is absorbed, the catalyst is filtered off. The filtrate is evaporated under reduced pressure to give the title compound (7 g) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870074 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-6913707d6d5a4a51b311a2425cfcfefa |
| Source note | uspto-grants-1989_09 |