HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 54447535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | (Triphenylphosphoranylidene)acetaldehyde | HCID 75051 | — |
| Reactant | HCID 14877943 | HCID 14877943 | — |
| Product | HCID 54447535 | HCID 54447535 | 85% |
Reaction Steps
Following the general procedure of Example 7, 3.8 g (11.6 mmoles) of 3,3-bis(4-fluorophenyl)-2-(5-methyl-1H-tetrazol-1-yl)-2-propenal in 200 mL of dry benzene was treated with 3.8 g (12.5 mmoles) of triphenylphosphoranylidene acetaldehyde to produce 3.5 g (85%) of the title compound; m.p.=72°-78° C. (foam).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870187 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-8fe786664aaf415a9d297089982edf2f |
| Source note | uspto-grants-1989_09 |