HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53685369, compound → HCID 54375809, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53685369 | HCID 53685369 | — |
| Reactant | HCID 73668863 | HCID 73668863 | — |
| Product | HCID 54375809 | HCID 54375809 | 63% |
Reaction Steps
The general procedure of Example 9 was repeated except that the ethyl 9,9-bis(4-fluorophenyl)-5-hydroxy-8-(5-phenyl-1H-tetrazol-1-yl)-3-oxo-6,8-nonadienoate utilized therein was replaced by 2.0 g of 9,9-bis(4-fluorophenyl)-5-hydroxy-8-(5-methyl-1H-tetrazol-1-yl)-3-oxo-6,8-nonadienoate and there was thereby produced 1.25 g (63%) of the title compound after purification by silica gel column chromatography with ethyl acetate in hexanes as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870187 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-c4934542a58b4d658cae84791bac9afc |
| Source note | uspto-grants-1989_09 |