Allyl bromide → HCID 53959466, compound

Participants

Reaction Steps

Substantially the same procedure as in Reference Example 3 was repeated using 300 mg (0.90 mmol) of 6-amino-5-(3-tricyclo[3.3.1.03,7 ]nonylcarbonylamino)-1-propyluracil (Japanese Published Unexamined Patent Application No. 173889/91) and 0.16 ml (1.81 mmol) of allyl bromide. The obtained crude product was subjected to the same cyclization reaction that was used in Example 1, without purification, to give 110 mg (yield 35%) of Compound J as a white powder.

Provenance & Evidence