HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Dinitroazetidine → 3,3-Dinitroazetidinium 2,4-dinitroimidazolate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Dinitroazetidine | HCID 5231706 | — |
| Reactant | HCID 178526857 | HCID 178526857 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 3,3-Dinitroazetidinium 2,4-dinitroimidazolate | HCID 131718918 | 95% |
Reaction Steps
3,3-Dinitroazetidine free base (1.0 g) was added to a solution of 2,4-dinitroimidazole (1.07 g) in 50 ml of warm acetonitrile. The solution was allowed to cool and the majority of the solvent evaporated. The remaining slurry was filtered and dried to give 1.98 g of the resultant product, 3,3-dinitroazetidinium 2,4-dinitroimidazolate (95% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05395945 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-f2cc1d08b8f14befacdfcb47b96c50ce |
| Source note | uspto-grants-1995_03 |