HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → (Hexahydro-1H-furo[3,4-c]pyrrol-3a-yl)methanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 22924372 | HCID 22924372 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | (Hexahydro-1H-furo[3,4-c]pyrrol-3a-yl)methanamine | HCID 19960957 | — |
Reaction Steps
2.8 g (12.1 mmol) of 1-aminomethyl-7-azabicyclo[3.3.0]octane are dissolved in 50 ml of ethanol and hydrogenated on 0.3 g of palladium-active charcoal at 100° C. and 100 bar. The catalyst is filtered off with suction and the filtrate is concentrated and distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05395944 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-0e0aef67e0394252bb0e6735a627bdb6 |
| Source note | uspto-grants-1995_03 |