HuagongsheHuagongshe Chemistry Print Report · For research reference only
AC1LBHMA → HCID 20082685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | AC1LBHMA | HCID 582874 | — |
| Reactant | 4-(4-Chlorophenyl)-1-butene | HCID 11052032 | — |
| Product | HCID 20082685 | HCID 20082685 | 70.8% |
Reaction Steps
About 33.3 g (0.2 mol) of 4-(3-butenyl)-1-chlorobenzene prepared in accordance with Example 1 (b) were silylated with 2,4,4-trimethyl-2,4-disilapentane (compare Example 1 (d) with Pt as catalyst to give 1-chloro-4-(5,5,7,7-tetramethyl-5,7disilaoctyl)benzene. The boiling point was 115° C. under 0.05 hPa, and the yield was 70.8% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05399290 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-0aa7fe9bcf794aa19bb62a6832ad44df |
| Source note | uspto-grants-1995_03 |