HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl isocyanate → HCID 54106829, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl isocyanate | HCID 76639 | — |
| Reactant | 2-Butanol, 1-[3-(trifluoromethyl)phenoxy]- | HCID 11379302 | — |
| Catalyst | Triethylamine | HCID 8471 | — |
| Solvent | Hexane | HCID 8058 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54106829 | HCID 54106829 | — |
Reaction Steps
4.7 g of 1-(3-trifluoromethylphenoxy)-butan-2-ol and 2.7 g of benzyl isocyanate are dissolved in 60 ml of ethyl acetate. After addition of one drop of triethylamine, the reaction mixture is allowed to stand for 20 hours at 22° C. The solvent is stripped off and the residue is stirred in n-hexane. The desired crystalline product, O--[1-(3-trifluoromethylphenoxy)-2-butyl]-N-benzylcarbamate, is obtained in a yield of 5.2 g; m.p. 73°-74° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05399545 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-bc826bfa28d6435793d174bae07e4fd6 |
| Source note | uspto-grants-1995_03 |