Hydrochloric Acid → HCID 53758662, compound

HRID 1609119Notes

Reaction equation

HRID 1609119 reaction equation
[CH2:1](Br)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH:10]=[CH2:11].[CH3:13][NH:14][CH3:15].Cl>>[CH3:13][N:14]([CH3:15])[CH:4]([CH2:3][CH2:2][CH3:1])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH:10]=[CH2:11]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 674DimethylamineHCID 28414811-Bromo-1-undecene

Product 1

HCID 53758662HCID 53758662, compound

Conditions

Temperature
20 °C

Procedure

A mixture of 96.49 g of undecylenyl bromide and 314.0 ml of dimethylamine is agitated for 48 hours at 20° C. At the end of the reaction, the pH is brought to 2 by a hydrochloric acid solution (10%). The amine is extracted with methylene chloride.

Workup

  1. customAt the end of the reaction
  2. extractionThe amine is extracted with methylene chloride

Sources & evidence

ORD record
ord-f193ca349a304ecb854252b42ae0045c
Source dataset
uspto-grants-1995_03
Patent number
US05399590

Reaction notes

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