4-Methylbenzyl alcohol → HCID 20084145, compound

Participants

Reaction Steps

12.21 g (0.1 mol) of 4-methylbenzylalcohol and 35.78 g (0.1 mol) of N,N-dimethylaniline hexafluoroantimonate were dissolved in 100 g of nitromethane and allowed to react at 80° C. for 8 hours. After the completion of the reaction, the mixture was concentrated, and the precipitated white solid was washed with ether and dried to give the titled compound. Yield: 55%.

Provenance & Evidence