HuagongsheHuagongshe Chemistry Print Report · For research reference only
Paeonol → HCID 10085417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Paeonol | HCID 11092 | — |
| Reactant | 2-Chlorobenzoyl chloride | HCID 69110 | — |
| Product | HCID 10085417 | HCID 10085417 | — |
Reaction Steps
2 is prepared from 2-hydroxy-4-methoxyacetophenone and 2-chlorobenzoyl chloride by the procedure of Example 1. Material is purified by flash chromatography (gradient elution using 25% ethyl acetate in hexane and 10% ethyl acetate in chloroform; material is loaded on column in methylene chloride), yielding 2 with a melting point of 148.5°-149.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05399584 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-70ace0029b044108ad4bd4b9faa27457 |
| Source note | uspto-grants-1995_03 |