HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha-Hydroxyacetophenone → HCID 776385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha-Hydroxyacetophenone | HCID 68490 | — |
| Reactant | 2-Methylbenzoyl chloride | HCID 70276 | — |
| Product | HCID 776385 | HCID 776385 | — |
Reaction Steps
7 is prepared from 2-methylbenzoyl chloride (8) and 2-hydroxyacetophenone by the procedure of Example 1. The material is purified by vacuum column (eluting with 10% ethyl acetate in hexane), yielding 7 with a melting point of 45.5°-47.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05399584 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-9d226149205e428da9ef06116dc8a5e7 |
| Source note | uspto-grants-1995_03 |