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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1609260Generated: October 30, 2026

Potassium Carbonate → Ethyl 2-[3-(2-nitrophenoxy)phenoxy]propionate

https://huagongshe.com/reaction/1609260

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantEthyl 2-bromopropionateHCID 79040—
Reactant3-(2-Nitrophenoxy)phenolHCID 12588693—
SolventAcetoneHCID 180—
ProductEthyl 2-[3-(2-nitrophenoxy)phenoxy]propionateHCID 20084526101.2%

Reaction Steps

In 120 ml of acetone were dissolved 8.0 g of 3-(2-nitrophenoxy)phenol and 7.5 g of ethyl 2-bromopropionate followed by addition of 7.2 g of potassium carbonate. The mixture was refluxed for 5 hours and, after cooling, the insoluble matter was filtered off. The filtrate was concentrated to give 11.6 g of the title compound as a light brown oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05399703
Source datasetuspto-grants-1995_03
ORD IDord-0971f6ca9b15434b9dd4136ee6ca352c
Source noteuspto-grants-1995_03