HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Ethyl 2-[3-(2-nitrophenoxy)phenoxy]propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 2-bromopropionate | HCID 79040 | — |
| Reactant | 3-(2-Nitrophenoxy)phenol | HCID 12588693 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Ethyl 2-[3-(2-nitrophenoxy)phenoxy]propionate | HCID 20084526 | 101.2% |
Reaction Steps
In 120 ml of acetone were dissolved 8.0 g of 3-(2-nitrophenoxy)phenol and 7.5 g of ethyl 2-bromopropionate followed by addition of 7.2 g of potassium carbonate. The mixture was refluxed for 5 hours and, after cooling, the insoluble matter was filtered off. The filtrate was concentrated to give 11.6 g of the title compound as a light brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05399703 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-0971f6ca9b15434b9dd4136ee6ca352c |
| Source note | uspto-grants-1995_03 |