HRID1609260

反应详情

EQUATION

反应方程式

HRID 1609260 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In 120 ml of acetone were dissolved 8.0 g of 3-(2-nitrophenoxy)phenol and 7.5 g of ethyl 2-bromopropionate followed by addition of 7.2 g of potassium carbonate. The mixture was refluxed for 5 hours and, after cooling, the insoluble matter was filtered off. The filtrate was concentrated to give 11.6 g of the title compound as a light brown oil.

WORKUP

后处理

  1. temperatureThe mixture was refluxed for 5 hours
  2. temperatureafter cooling
  3. filtrationthe insoluble matter was filtered off
  4. concentrationThe filtrate was concentrated