HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178526592, compound → HCID 178507514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178526592 | HCID 178526592 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178507514 | HCID 178507514 | 96.9% |
Reaction Steps
In a mixture of 18 ml of ethanol and 9 ml of N,N-dimethylformamide was dissolved 1.5 g of 5-[3-(2-nitrophenoxy)phenyl]-1H-tetrazole and catalytic hydrogenation was carried out in the presence of 0.3 g of palladium-carbon at atmospheric temperature and pressure. After this reaction, the catalyst was filtered off and the filtrate was concentrated to give 1.3 g of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05399703 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-3cd4713068c648a68992414b5474dcf2 |
| Source note | uspto-grants-1995_03 |