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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1609268Generated: October 30, 2026

HCID 178526592, compound → HCID 178507514, compound

https://huagongshe.com/reaction/1609268

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178526592HCID 178526592—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
SolventDimethylformamideHCID 6228—
ProductHCID 178507514HCID 17850751496.9%

Reaction Steps

In a mixture of 18 ml of ethanol and 9 ml of N,N-dimethylformamide was dissolved 1.5 g of 5-[3-(2-nitrophenoxy)phenyl]-1H-tetrazole and catalytic hydrogenation was carried out in the presence of 0.3 g of palladium-carbon at atmospheric temperature and pressure. After this reaction, the catalyst was filtered off and the filtrate was concentrated to give 1.3 g of the title compound as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05399703
Source datasetuspto-grants-1995_03
ORD IDord-3cd4713068c648a68992414b5474dcf2
Source noteuspto-grants-1995_03