Methyl iodide → HCID 20084491, compound

Participants

Reaction Steps

In 20 ml of N,N-dimethylformamide was dissolved 2.8 g of 2-[2-(trifluoroacetylamino)phenylthio]benzonitrile followed by addition of 2.4 g of methyl iodide and 2.4 g of potassium carbonate, and the mixture was stirred at room temperature for 2 hours, at the end of which time the reaction mixture was diluted with water. The crystals separated out therefrom were collected by filtration, washed with water and aqueous ethanol to give 2.8 g of the title compound as white crystals.

Provenance & Evidence