Sodium Hydroxide → HCID 20084552, compound

Participants

Reaction Steps

In 20 ml of ethanol was suspended 2.8 g of 2-[2-(N-methyl-N-trifluoroacetylamino)phenylthio]benzonitrile followed by addition of 4 ml of 10% aqueous sodium hydroxide solution, and the mixture was heated on a water bath for 5 minutes. After cooling, the crystals were collected by filtration and washed with 50% aqueous ethanol to give 1.8 g of the title compound as white crystals.

Provenance & Evidence