HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → Triphenylphosphine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 4-Chloromethyl-2-cyclobutyl-thiazole | HCID 18759094 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Triphenylphosphine hydrochloride | HCID 9882740 | — |
Reaction Steps
A mixture of 4.8 g of 4-chloromethyl-2-cyclobutyl-thiazole, 7.0 g of triphenylphosphine and 125 ml of toluene was heated to reflux for 16 hr and then cooled to room temperature. The mixture was then filtered to yield 4.8 g of [(2-cyclobutyl-4-thiazolyl)methyl]=triphenylphosphonium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05399702 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-9457bf3dd4c5472484bcc43448dfd73a |
| Source note | uspto-grants-1995_03 |