HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 22814771, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | delta-Gluconolactone | HCID 7027 | — |
| Solvent | Isopropanol methanol | HCID 21255859 | — |
| Product | HCID 22814771 | HCID 22814771 | — |
Reaction Steps
A suspension of 50 g gluconolactone in 500 ml of isopropanol/methanol (4/1) was treated with 23.8 ml of a 40% N-methylamine solution for 30 minutes. The N-methylgluconamide obtained in quantitative yields, was treated at 60° C. with 69 ml acetic anhydride and 35 ml acetic acid in the presence of 1% concentrated sulphuric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05401435 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-37ece4a4b5bd4990a6ee9924cd3108bc |
| Source note | uspto-grants-1995_03 |