Pyridine → HCID 20081443, compound

Participants

Reaction Steps

Acetyl chloride (0.35 g) was added to a stirred, cooled mixture of the product of Example 1 (1.5 g) and pyridine (0.39 g) in dichloromethane (20 ml). Stirring was continued for 2 hours and the mixture was allowed to stand overnight. The organic solution was washed with water (twice), dried over magnesium sulfate and run down under vacuum. The residue was triturated with ether to yield a white solid, 0.38 g (23%), mp 100°-101.5° C.

Provenance & Evidence