Cyclohexylamine → HCID 67780747, compound

Participants

Reaction Steps

A solution of the product of Example 1 (1.0 g) in ether (35 ml) was treated dropwise, with stirring and cooling, with cyclohexylamine (0.3 g) in ether (7 ml). The mixture was stirred for one hour and allowed to stand overnight at room temperature. The precipitated salt was filtered off, washed with ether and dried, yielding 1.15 g (88%), mp 158°-160° C.

Provenance & Evidence