L-Aspartic Acid → HCID 9837063, compound

Participants

Reaction Steps

L-aspartic acid (2.00 g, 15.0 mmol) was added to an MeOH solution of NaOMe (prepared with Na: 0.69 g, MeOH: 50 ml) at 0° C. and stirred. An MeOH solution (30 ml) of zinc acetate dihydrate (3.30 g) was then gradually dropwise added thereto at room temperature. After stirring for 2 hours at that same temperature, the precipitated crystal (in suspension) was recovered by filtration, washed with water, air dried, and then dried under a reduced pressure (5 mmHg, 80° C.).

Provenance & Evidence