L-Glutamic Acid → HCID 86605461, compound

Participants

Reaction Steps

L-glutamic acid (2.0 g, 13.6 mmol) was added to an MeOH solution of NaOMe (prepared with Na: 0.31 g, MeOH: 50 ml) at 0° C. and stirred. An MeOH solution (30 ml) of zinc acetate dihydrate (1.49 g) was then slowly dropwise added thereto. After refluxing and stirring for 5 hours, the precipitated crystal (in suspension) was recovered by filtration, washed with water, air dried, and then dried under a reduced pressure (5 mmHg, 80° C.).

Provenance & Evidence