L-Valine → HCID 86748589, compound

Participants

Reaction Steps

L-valine (2.00 g, 17.1 mmol) was added to an MeOH solution of NaOMe (prepared with Na: 0.39 g, MeOH: 50 ml) at 0° C. and stirred. An MeOH solution (30 ml) of zinc acetate dihydrate (1.90 g) was then slowly dropwise added thereto at room temperature. After stirring for 6 hours at that same temperature, the precipitated crystal (in suspension) recovered by filtration, washed with water, air dried, and then dried under a reduced pressure (5 mmHg, 80° C.).

Provenance & Evidence