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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1609616Generated: October 30, 2026

HCID 18648568, compound → HCID 53977342, compound

https://huagongshe.com/reaction/1609616

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18648568HCID 18648568—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 53977342HCID 53977342—

Reaction Steps

1.1 g of N-(1-carboethoxy-3-benzoxycarbonylaminopropyl)-L-alanyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid are dissolved in 150 ml of methanol and are hydrogenated in the presence of 100 mg of palladium/active charcoal (10% strength) at 40° C. under normal pressure. After the end of the reaction, the solution is filtered off from the catalyst and the solvent is stripped off in vacuo. Yield: 0.79 g

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05401766
Source datasetuspto-grants-1995_03
ORD IDord-14303befa9334bc396bd7646b1c949a4
Source noteuspto-grants-1995_03