m-Chloroperbenzoic acid → HCID 53697930, compound

HRID 1609640Notes

Reaction equation

HRID 1609640 reaction equation
ClC1C=CC=C(C(OO)=[O:9])C=1.[F:12][C:13]1[CH:21]=[C:20]2[C:16]([C:17]([CH2:33][C:34]([OH:36])=[O:35])=[C:18]([CH3:32])[C:19]2=[CH:22][C:23]2[CH:28]=[CH:27][C:26]([S:29]([CH3:31])=[O:30])=[CH:25][CH:24]=2)=[CH:15][C:14]=1[O:37][CH3:38]>CC(C)=O>[F:12][C:13]1[CH:21]=[C:20]2[C:16]([C:17]([CH2:33][C:34]([OH:36])=[O:35])=[C:18]([CH3:32])[C:19]2=[CH:22][C:23]2[CH:28]=[CH:27][C:26]([S:29]([CH3:31])(=[O:9])=[O:30])=[CH:25][CH:24]=2)=[CH:15][C:14]=1[O:37][CH3:38]

Participants

4

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 53670423HCID 53670423, compound

Product 1

HCID 53697930HCID 53697930, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

6-Fluoro-5-methoxy-2-methyl-1-(ρ-methylsulfonylbenzylidene)-3-indenyl acetic acid is prepared according to the procedure of Example 7 by the addition of 1.0 mole of m-chloroperbenzoic acid per mole of 6-fluoro-5-methoxy-2-methyl-1-(ρ-methylsulfinylbenzylidene)-3-indenyl acetic acid in an acetone solution.

Sources & evidence

ORD record
ord-ec03a1e34331457188c424362b90a34d
Source dataset
uspto-grants-1995_03
Patent number
US05401774

Reaction notes

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