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HRID1609715

反应详情

EQUATION

反应方程式

HRID 1609715 的结构方程式

REACTANTS

反应物

1
结构：COc1ccc(Oc2c(C)cc([N+](=O)[O-])cc2C)cc1C(C)C
HCID10313602

2-[4-Methoxy-3-(1-methylethyl)phenoxy]-1,3-dimethyl-5-nitrobenzene

C18H21NO4

PRODUCTS

生成物

1
结构：COc1ccc(Oc2c(C)cc(N)cc2C)cc1C(C)C
HCID10016799

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pt]
催化剂HCID23939

Platinum

Pt

结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

3,5-Dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)-nitrobenzene (6.0 g) and 600 mg of 10% platinum on carbon in 200 ml ethanol are hydrogenated on a Parr shaker. Catalyst is removed by filtration through Celite and the filtrate is stripped to afford 3,5-dimethyl4-(3'-isopropyl-4'-methoxyphenoxy)-aniline.

WORKUP

后处理

  1. customCatalyst is removed by filtration through Celite