HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+-)-2-Butanol → Sec-Butyl Propanoyloxymethyl Carbonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+-)-2-Butanol | HCID 6568 | — |
| Reactant | Propanoyloxymethyl Carbonochloridate | HCID 14800977 | — |
| Product | Sec-Butyl Propanoyloxymethyl Carbonate | HCID 20082466 | — |
Reaction Steps
A mixture of 2-butanol (0.092 mL, 1 mmol), 7c (0.17 g, 1 mmol), and powdered molecular sieve (0.15 g, 4Å) in alcohol-free CHCl3 (2 mL) is refluxed for 18 h. Following filtration through filter-aid and evaporation 0.2 g (98%) of the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05401868 |
| Source dataset | uspto-grants-1995_03 |
| ORD ID | ord-c381f5bef7a84f6c953e96cd013b9ce5 |
| Source note | uspto-grants-1995_03 |