Hydrochloric Acid → 2-Amino-7-(2-ethoxycarbonyl)vinyl-tetraline hydrochloride

HRID 1609780Notes

Reaction equation

HRID 1609780 reaction equation
C(OC([NH:8][CH:9]1[CH2:18][CH2:17][C:16]2[C:11](=[CH:12][C:13]([CH:19]=[CH:20][C:21]([O:23][CH2:24][CH3:25])=[O:22])=[CH:14][CH:15]=2)[CH2:10]1)=O)(C)(C)C.[ClH:26]>C(O)C>[ClH:26].[NH2:8][CH:9]1[CH2:18][CH2:17][C:16]2[C:11](=[CH:12][C:13]([CH:19]=[CH:20][C:21]([O:23][CH2:24][CH3:25])=[O:22])=[CH:14][CH:15]=2)[CH2:10]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 542570882-Tertbutoxycarbonylamino-7-(2-ethoxycarbonyl)vinyl-tetraline

Product 1

HCID 677818702-Amino-7-(2-ethoxycarbonyl)vinyl-tetraline hydrochloride

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of the compound obtained in step d) above (2.7 g, 0.0078 mol) in absolute ethanol (50 ml) is allowed to react at room temperature for 5 hours with 4N HCl absolute ethanol (33 ml).

Sources & evidence

ORD record
ord-f51f127c3ff24a89a097fb9c66aba5a8
Source dataset
uspto-grants-1995_03
Patent number
US05401879

Reaction notes

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