HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Hydrogenmaleate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Maleic Acid | HCID 444266 | — |
| Reactant | (1r,2r)-2-(1-Methylhydrazino)-1-indanol | HCID 9857292 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Hydrogenmaleate | HCID 87460142 | — |
Reaction Steps
(1R,2R)-2-(1-methylhydrazino)-1-indanol (1.45 g, 8.1 mmol, prepared from (1R,2R)-2-methylamino-1-indanol (1.63 g, 10 mmol) according to Example 1) was treated with an equivalent amount of maleic acid in a mixture of EtOH and Et2O to give crystalline hydrogenmaleate salt which was filtered off and recrystallized.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06982286B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-07c6fb5e639c43e5a2d031433f9a75b8 |
| Source note | uspto-grants-2006_01 |