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HRID1610027

反应详情

EQUATION

反应方程式

HRID 1610027 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CCOC(=O)[C@@H](N)CS
HCID13359

Ethyl L-cysteinate

C5H11NO2S

结构：COc1ccc(C#N)c(OC)c1
HCID77750

2,4-Dimethoxybenzonitrile

C9H9NO2

PRODUCTS

生成物

1
结构：CCOC(=O)[C@@H]1CSC(c2ccc(OC)cc2OC)=N1
HCID17747724

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

2,4-Dimethoxybenzonitrile, (R)-cysteine ethyl ester and about 5 equivalents of triethylamine are refluxed in ethanol for about 6–8 hours to obtain ethyl-2-(2,4-dimethoxyphenyl)-4,5-dihydro-thiazole-4-(R)-carboxylate.