Diethylamine → 4-Bromo-N,N-diethyl-2-fluorobenzamide

HRID 16103Notes

Reaction equation

[Br:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=O)=[C:4]([F:11])[CH:3]=1.[CH2:12]([NH:14][CH2:15][CH3:16])[CH3:13]>>[Br:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([N:14]([CH2:15][CH3:16])[CH2:12][CH3:13])=[O:8])=[C:4]([F:11])[CH:3]=1

Participants

Reactant 2

HCID 8021Diethylamine

HCID 3026814-Bromo-2-fluorobenzoic acid

Product 1

HCID 246940264-Bromo-N,N-diethyl-2-fluorobenzamide

Procedure

The sub-title compound was prepared by the method of example 18 step a) using 4-bromo-2-fluorobenzoic acid and N-ethyl-ethanamine.

Sources & evidence

ORD record: ord-f74797b5c1ae4c5b8d28a3cb3eb02fc1
Source dataset: uspto-grants-2010_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07737135B2

Reaction notes

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