HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 22258244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 22258232 | HCID 22258232 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 22258244 | HCID 22258244 | — |
Reaction Steps
The compound is prepared as described in example XVII with 1.00 g (6.66 mmol) 2,4-Dimethyl-4,5,6,7-tetrahydro-1H-benzimidazole (example XI, step 1), 3.09 g (21.97 mmol) of benzoyl chloride and 2.36 g (23.30 mmol) of TEA in 20 ml acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06984646B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-ac8aea67fe11455f8935b573deef973d |
| Source note | uspto-grants-2006_01 |