HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propiolic Acid → HCID 22258272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propiolic Acid | HCID 10110 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 22258258 | HCID 22258258 | — |
| Product | HCID 22258272 | HCID 22258272 | — |
Reaction Steps
The compounds are prepared as described in example 10 with 200 mg (0.70 mmol) of 2-(5,6-Dimethyl-4,5,6,7-tetrahydro-1H-benzimidazol-2-yl)-1-(4-fluorophenyl)ethanone (example XIV), 73.3 mg (1.05 mmol) of propiolic acid and 204 mg (1.26 mmol) of 1-(1H-imidazol-1-ylcarbonyl)-1H-imidazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06984646B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-6e2be6ba9a34476399ee578377b5d8cb |
| Source note | uspto-grants-2006_01 |