HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dichloroacetone → HCID 22259331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dichloroacetone | HCID 10793 | — |
| Reactant | HCID 22259286 | HCID 22259286 | — |
| Product | HCID 22259331 | HCID 22259331 | 41.9% |
Reaction Steps
Using (E)-3-(4-chloro-3-fluorophenyl)-2-propenamide (8.67 g) and 1,3-dichloroacetone (11.0 g), the same reaction as Reference Example 1-(ii) was carried out to yield the titled compound (4.95 g) as colorless flaky crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06984653B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-2ecf40f2f4e449c2bb3a6293d80ae2b2 |
| Source note | uspto-grants-2006_01 |