HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanesulfonyl chloride → HCID 22259307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanesulfonyl chloride | HCID 82408 | — |
| Reactant | HCID 22259339 | HCID 22259339 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 22259307 | HCID 22259307 | — |
Reaction Steps
Using 2-[1-[4-[4-[[2-[(E)-2-[4-(trifluoromethyl)phenyl]ethenyl]-1,3-oxazol-4-yl]methoxy]phenyl]butyl]-1H-imidazol-2-yl]ethylamine (248 mg), triethylamine (135 μl) and 2-propanesulfonyl chloride (65.5 μl), the same reaction as Example 31 was carried out to yield the titled compound (55 mg) as colorless needle crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06984653B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-23312ace0e8a4ed0aa331ce4108f5528 |
| Source note | uspto-grants-2006_01 |