HCID 22259882, compound → 41331-11-7

HRID 1611075Notes

Reaction equation

HRID 1611075 reaction equation
Cl.[CH2:2]([NH:8][CH2:9][CH2:10][C:11]([O:13]C)=[O:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]>Cl>[CH2:2]([NH:8][CH2:9][CH2:10][C:11]([OH:13])=[O:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]

Participants

3

Reactant 1

HCID 22259882HCID 22259882, compound

Product 1

HCID 1384843741331-11-7

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

Methyl 3-(1-hexylamino)propionate hydrochloride (see Example 2 for preparation) was hydrolyzed by refluxing in 2N HCl for 24 hours followed by evaporation to dryness; m.p.=95-97° C. (no lit. value).

Workup

  1. customfollowed by evaporation to dryness

Sources & evidence

ORD record
ord-7aa5ae0337704a4d94f0aeeb9045d035
Source dataset
uspto-grants-2006_01
Patent number
US06984754B1

Reaction notes

Loading…