HCID 23591244, compound → HCID 86599715, compound

Participants

Reaction Steps

A solution of (R)-diethyl 2-(2-heptylamino)ethanephosphonate hydrochloride (0.19 g, 0.68 mmol) in concentrated HCl (7 mL) was heated at 90° C. for 48 hours. The reaction mixture was then evaporated to dryness and the residue triturated with acetone. The white solid was filtered and air-dried giving an 86% overall yield; m.p.=106-112° C. (no lit. value).

Provenance & Evidence