1,2-Dimethoxyethane → HCID 5259923, compound

HRID 1611096Notes

Reaction equation

HRID 1611096 reaction equation
[Ti:1]([Cl:5])([Cl:4])([Cl:3])[Cl:2].[CH3:6][O:7][CH2:8][CH2:9][O:10][CH3:11]>ClCCl>[CH3:6][O:7][CH2:8][CH2:9][O:10][CH3:11].[Ti:1]([Cl:5])([Cl:4])([Cl:3])[Cl:2]

Participants

4

Reactant 2

HCID 80711,2-DimethoxyethaneHCID 24193Titanium Tetrachloride

Product 1

HCID 5259923HCID 5259923, compoundYield 86%

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

A solution of 19 g (100 mmol) of titanium tetrachloride in 250 ml of dichloromethane is admixed at 0° C. with 9.0 g (100 mmol) of 1,2-dimethoxyethane and stirred at room temperature for another 1 hour. The solvent is subsequently taken off, giving 24 g (86%) of titanium tetrachloride-(1,2-dimethoxyethane) adduct as a yellow solid.

Sources & evidence

ORD record
ord-edf628f021a8421cb43cec54b78c8a22
Source dataset
uspto-grants-2006_01
Patent number
US06984743B1

Reaction notes

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