HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dimethoxyethane → HCID 5259923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dimethoxyethane | HCID 8071 | — |
| Reactant | Titanium Tetrachloride | HCID 24193 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 5259923 | HCID 5259923 | 86% |
Reaction Steps
A solution of 19 g (100 mmol) of titanium tetrachloride in 250 ml of dichloromethane is admixed at 0° C. with 9.0 g (100 mmol) of 1,2-dimethoxyethane and stirred at room temperature for another 1 hour. The solvent is subsequently taken off, giving 24 g (86%) of titanium tetrachloride-(1,2-dimethoxyethane) adduct as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06984743B1 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-edf628f021a8421cb43cec54b78c8a22 |
| Source note | uspto-grants-2006_01 |