HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Chloromethyl)anthraquinone → 6-(3,5-Dimethylphenyl)sulfanyl-1-[(9,10-dioxo-2-anthryl)methyl]-5-isopropyl-pyrimidine-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Chloromethyl)anthraquinone | HCID 344311 | — |
| Reactant | 5-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedione | HCID 10493727 | — |
| Product | 6-(3,5-Dimethylphenyl)sulfanyl-1-[(9,10-dioxo-2-anthryl)methyl]-5-isopropyl-pyrimidine-2,4-dione | HCID 15957780 | 32.2% |
Reaction Steps
5-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedione and 2-chloromethyl anthraquinone were reacted by the same way with the example 1 to obtain the titled compound (165 mg, yield: 32.2%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06987114B1 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-8acf8bf555884ac68292555536c2f908 |
| Source note | uspto-grants-2006_01 |