1-Bromo-2-butanone → HCID 15957829, compound

HRID 1611392Notes

Reaction equation

HRID 1611392 reaction equation
[CH2:1]([C:3]1[C:4](=[O:19])[NH:5][C:6](=[O:18])[NH:7][C:8]=1[O:9][C:10]1[CH:15]=[C:14]([CH3:16])[CH:13]=[C:12]([CH3:17])[CH:11]=1)[CH3:2].Br[CH2:21][C:22](=[O:25])[CH2:23][CH3:24]>>[CH2:21]([N:7]1[C:8]([O:9][C:10]2[CH:11]=[C:12]([CH3:17])[CH:13]=[C:14]([CH3:16])[CH:15]=2)=[C:3]([CH2:1][CH3:2])[C:4](=[O:19])[NH:5][C:6]1=[O:18])[C:22](=[O:25])[CH2:23][CH3:24]

Participants

3

Reactant 2

HCID 131561-Bromo-2-butanoneHCID 109232665-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione

Product 1

HCID 15957829HCID 15957829, compoundYield 56%

Procedure

5-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione and 1-bromo-2-butanone were reacted by the same way with the example 1 to obtain the titled compound (185 mg, yield: 56%).

Sources & evidence

ORD record
ord-4dc293e39e2d41b7b35a9efa9bb174c5
Source dataset
uspto-grants-2006_01
Patent number
US06987114B1

Reaction notes

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