HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 15289174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 15289172 | HCID 15289172 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15289174 | HCID 15289174 | 73% |
Reaction Steps
200 mg of compound (23) are dissolved in 20 ml of MeOH. Adding 8 mg of K2CO3 results in hydrolysis after 1 h of stirring. After the solution has been subjected to rotary evaporation, the residue is chromatographed on silica gel in the eluent methylene chloride/MeOH (8:1). Recrystallization from MeOH results in colorless crystals (73%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06987177B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-6832528897e14d89ac28cf9f22f6a56f |
| Source note | uspto-grants-2006_01 |