4-Methoxyphenol → HCID 86601934, compound

HRID 1611569Notes

Reaction equation

HRID 1611569 reaction equation
[Na:1].S(CCC[CH2:9][O:10][C:11]1[CH:16]=[CH:15][C:14]([O:17][CH2:18][CH2:19][CH2:20]CS(O)(=O)=O)=[CH:13][CH:12]=1)(O)(=O)=O.COC1C=CC(O)=CC=1.C1[S:40](=[O:42])(=[O:41])[O:39]CCC1.[Na].COC1C=CC=CC=1OCCCCS(O)(=O)=O>>[Na:1].[CH3:9][O:10][C:11]1[CH:12]=[CH:13][C:14]([O:17][CH2:18][CH2:19][CH2:20][S:40]([OH:42])(=[O:41])=[O:39])=[CH:15][CH:16]=1

Participants

5

Reactant 4

HCID 90154-MethoxyphenolHCID 154111,4-Butane sultoneHCID 86601936HCID 86601936, compoundHCID 86601937HCID 86601937, compound

Product 1

HCID 86601934HCID 86601934, compound

Procedure

In the same manner as in above (1), the objective compound was synthesized from 4-methoxyphenol and butanesultone. The crude product was recrystallized from water to obtain a milky white needle crystal product. The resulting product was determined for its 1H-NMR and IR spectrum to confirm that it was 1-methoxy-4-sulfobutoxybenzene sodium.

Workup

  1. customThe crude product was recrystallized from water
  2. customto obtain a milky white needle crystal product

Sources & evidence

ORD record
ord-1732c4ea6c394b48ad82904c29616c05
Source dataset
uspto-grants-2006_01
Patent number
US06989212B2

Reaction notes

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