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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1611682Generated: October 31, 2026

Ammonia → HCID 10453036, compound

https://huagongshe.com/reaction/1611682

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
Reactant3,5-DichlorophenolHCID 11571—
Reactant2-Methyl-8-hydroxyquinolineHCID 13224—
ProductHCID 10453036HCID 10453036—

Reaction Steps

The title compound was prepared according to the procedure described in Example 86 substituting 3,5-dichlorophenol for 8-hydroxyquinaldine. 1H NMR (500 MHz, CDCl3) δ ppm 7.96 (d, 1H), 7.32 (t, 1H), 7.21 (dd, 1H), 7.12 (m, 1H), 6.99 (d, 1H), 6.84 (m, 1H), 6.64 (m, 2H), 4.68 (m, 1H), 4.05 (m, 1H), 3.95 (m, 1H), 2.18 (m, 1H), 2.00 (m, 3H), 1.47 (d, 3H); MS (DCI/NH3) m/z 391 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06989392B2
Source datasetuspto-grants-2006_01
ORD IDord-16f5166016134e259f6485241b5f4b00
Source noteuspto-grants-2006_01