HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 10453036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3,5-Dichlorophenol | HCID 11571 | — |
| Reactant | 2-Methyl-8-hydroxyquinoline | HCID 13224 | — |
| Product | HCID 10453036 | HCID 10453036 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 86 substituting 3,5-dichlorophenol for 8-hydroxyquinaldine. 1H NMR (500 MHz, CDCl3) δ ppm 7.96 (d, 1H), 7.32 (t, 1H), 7.21 (dd, 1H), 7.12 (m, 1H), 6.99 (d, 1H), 6.84 (m, 1H), 6.64 (m, 2H), 4.68 (m, 1H), 4.05 (m, 1H), 3.95 (m, 1H), 2.18 (m, 1H), 2.00 (m, 3H), 1.47 (d, 3H); MS (DCI/NH3) m/z 391 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06989392B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-16f5166016134e259f6485241b5f4b00 |
| Source note | uspto-grants-2006_01 |