Ammonia → HCID 10360329, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in Example 92 substituting 2-hydroxybenzonitrile for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, CDCl3) δ ppm 7.94 (d, 1H), 7.46 (m, 2H), 7.33 (t, 1H), 7.20 (m, 2H), 6.96 (m, 2H), 6.91 (m, 1H), 4.78 (m, 1H), 4.22 (m, 1H), 4.12 (m, 1H), 2.23 (m, 1H), 1.96–2.18 (m, 3H), 1.47 (d, 3H); MS (DCI/NH3) m/z 348 [M+H]+.

Provenance & Evidence