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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1611688Generated: November 2, 2026

Ammonia → HCID 10430315, compound

https://huagongshe.com/reaction/1611688

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
Reactant5-Amino-1-naphtholHCID 65746—
ReactantMethyl 3-HydroxybenzoateHCID 88068—
ProductHCID 10430315HCID 10430315—

Reaction Steps

The title compound was prepared according to the procedure described in Example 92 substituting 5-amino-1-naphthol for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, DMSO-d6) δ ppm 8.36 (d, 1H), 7.56 (d, 1H), 7.48 (m, 2H), 7.39 (m, 2H), 7.27 (t, 1H), 7.17 (m, 1H), 7.12 (d, 1H), 6.87 (d, 1H), 6.80 (d, 1H), 4.92 (m, 1H), 4.17 (m, 2H), 2.04 (m, 4H), 1.45 (d, 3H); MS (DCI/NH3) m/z 388 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06989392B2
Source datasetuspto-grants-2006_01
ORD IDord-a0fc0c74dcec4cbb848a2506034aabb0
Source noteuspto-grants-2006_01